(R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol

Base Information

• Chemical Name: (R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol
• CAS No.: 1122457-89-9
• Molecular Formula: C₄₉H₆₉NO₆Si₂
• Molecular Weight: 824.261

Synonyms:(R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol

Chemical Property of (R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol

Chemical Property:

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Technology Process of (R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol

There total 1 articles about (R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(hydroxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol (1062606-61-4) + tert-butylchlorodiphenylsilane (58479-61-1) → (R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol (1122457-89-9)

Guidance literature:

With 1H-imidazole; In dichloromethane; at -15 - 20 ℃;

DOI:10.1016/j.carres.2008.10.016

Reference yield: 84.0%

(R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol (1122457-89-9) + methanesulfonyl chloride (124-63-0) → (R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethyl mesylate (1122457-91-3)

Guidance literature:

With triethylamine; In dichloromethane; at -15 - 20 ℃;

DOI:10.1016/j.carres.2008.10.016

upstream raw materials:

(R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(hydroxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethanol

tert-butylchlorodiphenylsilane

Downstream raw materials:

(R)-2-(tert-butyldiphenylsilyloxy)-1-((2S,3S,3aS,4S,5S)-4,5-di-tert-butoxy-3-(tert-butyldiphenylsilyloxymethyl)hexahydropyrrolo[1,2-b]-isoxazol-2-yl)ethyl mesylate

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