(Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate

Base Information

• Chemical Name: (Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate
• CAS No.: 1450925-37-7
• Molecular Formula: C₂₃H₂₂N₂O₄
• Molecular Weight: 390.439
• Mol file: 1450925-37-7.mol

Synonyms:(Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate

Chemical Property of (Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate

There total 3 articles about (Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

4-hydroxy-N'-[(1Z)-1-(naphthalen-2-yl)ethylidene]benzohydrazide + ethyl bromoacetate (105-36-2) → (Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate (1450925-37-7)

Guidance literature:

With potassium carbonate; In acetone; for 24h; Reflux;

DOI:10.1016/j.jphotobiol.2013.02.014

Reference yield:

4-hydroxybenzoic acid hydrazide (5351-23-5) → (Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate (1450925-37-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / 8 h / 20 °C

2: potassium carbonate / acetone / 24 h / Reflux

With potassium carbonate; acetic acid; In acetone;

DOI:10.1016/j.jphotobiol.2013.02.014

Reference yield:

methyl 2-naphthyl ketone (93-08-3) → (Z)-ethyl 2-(4-(2-(1-(naphthalen-2-yl)ethylidene)hydrazinecarbonyl)phenoxy)acetate (1450925-37-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / 8 h / 20 °C

2: potassium carbonate / acetone / 24 h / Reflux

With potassium carbonate; acetic acid; In acetone;

DOI:10.1016/j.jphotobiol.2013.02.014

upstream raw materials:

4-hydroxybenzoic acid hydrazide

ethyl bromoacetate

methyl 2-naphthyl ketone