tricyclo[3.3.1.1~3,7~]decane-1,3-diyl dinitrate

Base Information

• Chemical Name: tricyclo[3.3.1.1~3,7~]decane-1,3-diyl dinitrate
• CAS No.: 53488-28-1
• Molecular Formula: C₁₀H₁₄N₂O₆
• Molecular Weight: 258.231
• Mol file: 53488-28-1.mol

Synonyms:dinitrate of 1,3-adamantanediol

Chemical Property of tricyclo[3.3.1.1~3,7~]decane-1,3-diyl dinitrate

Chemical Property:

• Vapor Pressure: 0.000158mmHg at 25°C

Purity/Quality:

98%min ^*data from raw suppliers

Tricyclo[3.3.1.1~3,7~]decane-1,3-diyl dinitrate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tricyclo[3.3.1.1~3,7~]decane-1,3-diyl dinitrate

There total 14 articles about tricyclo[3.3.1.1~3,7~]decane-1,3-diyl dinitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-nitroxyadamantane (32314-61-7) → dinitrate of 1,3-adamantanediol (53488-28-1)

Guidance literature:

With nitric acid; at 0 ℃; for 3h;

Reference yield: 80.0%

(1-Adamantyl)carbamidsaeure-methylester (59987-81-4) → dinitrate of 1,3-adamantanediol (53488-28-1)

Guidance literature:

With nitric acid; at 0 ℃; for 1h;

Reference yield: 59.0%

1,3-Difluoroadamantane (54043-61-7) → dinitrate of 1,3-adamantanediol (53488-28-1) + 3-fluoroadamantan-1-yl nitrate

Guidance literature:

With nitric acid; acetic anhydride; at 20 ℃; for 1h;

DOI:10.1134/S1070428020090055

upstream raw materials:

(1-adamantyl)dimethylamine

1-nitroxyadamantane

(1-Adamantyl)carbamidsaeure-methylester

1-Adamantyl bromide

Downstream raw materials:

adamantane-1,3-dicarboxylic acid

1,3-adamantane diacetic acid

1,3-Bis--adamantan

1,3-di(p-tolyl)tricyclo<3.3.1.1^3,7>decane