2,6-difluorobenzaldehyde propylene acetal

Base Information

Chemical Name:2,6-difluorobenzaldehyde propylene acetal
CAS No.:181305-64-6
Molecular Formula:C₁₀H₁₀F₂O₂
Molecular Weight:200.185
Hs Code.:

Synonyms:2,6-difluorobenzaldehyde propylene acetal

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Chemical Property of 2,6-difluorobenzaldehyde propylene acetal

Chemical Property:

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Technology Process of 2,6-difluorobenzaldehyde propylene acetal

There total 1 articles about 2,6-difluorobenzaldehyde propylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 437-81-0
2,6-difluorobenzaldehyde

: 504-63-2
trimethyleneglycol

: 181305-64-6
2,6-difluorobenzaldehyde propylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 2h; Heating;
DOI:10.1021/jm950639r

Reference yield:

: 181305-64-6
2,6-difluorobenzaldehyde propylene acetal

: 181305-69-1
2,6-difluoro-3-methoxymethylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, -70 deg C, 1 h, 2.) THF, hexane, RT, 18 h

2: 93 percent / 2M aq. HCl / dioxane / 70 h / Ambient temperature

With hydrogenchloride; n-butyllithium; In 1,4-dioxane;
DOI:10.1021/jm950639r

Reference yield:

: 181305-64-6
2,6-difluorobenzaldehyde propylene acetal

: 1026351-98-3
2,6-Difluoro-3-methoxymethylphenethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) THF, hexane, -70 deg C, 1 h, 2.) THF, hexane, RT, 18 h

2: 93 percent / 2M aq. HCl / dioxane / 70 h / Ambient temperature

3: 1.) NaOH, 2.) 4N aq. HCl / 1.) H₂O, methanol, -3 deg C, 15 min

4: 84 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jm950639r