N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid

Base Information

• Chemical Name: N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid
• CAS No.: 116140-07-9
• Molecular Formula: C₂₆H₃₃N₃O₄
• Molecular Weight: 451.566

Synonyms:N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid

Chemical Property of N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid

Chemical Property:

Purity/Quality:

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Technology Process of N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid

There total 2 articles about N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-isoleucine (73-32-5,959215-79-3,18875-42-8) → N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid (116140-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / 2N NaOH / dioxane; toluene / 0 °C

2: 87 percent / diethyl ether / 0.5 h / Ambient temperature

With sodium hydroxide; In 1,4-dioxane; diethyl ether; toluene;

DOI:10.1002/hlca.19880710118

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid (116140-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / 2N NaOH / dioxane; toluene / 0 °C

2: 87 percent / diethyl ether / 0.5 h / Ambient temperature

With sodium hydroxide; In 1,4-dioxane; diethyl ether; toluene;

DOI:10.1002/hlca.19880710118

Reference yield: 92.0%

N-(benzyloxycarbonyl)-L-isoleucyl-1-amino-N-methylcyclobutancarboxanilid (116140-07-9) → N-(benzyloxycarbonyl)-L-isoleucyl-1-aminocyclobutancarbonsaure (112142-83-3)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; for 58h; Ambient temperature;

DOI:10.1002/hlca.19880710118

upstream raw materials:

L-isoleucine

benzyl chloroformate

Downstream raw materials:

N-(benzyloxycarbonyl)-L-isoleucyl-1-aminocyclobutancarbonsaure

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