(3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one

Base Information

• Chemical Name: (3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one
• CAS No.: 177422-46-7
• Molecular Formula: C₂₈H₂₄O₈
• Molecular Weight: 488.494

Synonyms:(3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one

Chemical Property of (3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one

Chemical Property:

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Technology Process of (3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one

There total 5 articles about (3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

(5E)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one (177568-33-1) → (3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one (177422-46-7) + (3S,5R)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 12h; Yields of byproduct given;

DOI:10.1021/jo960042z

Reference yield: 40.0%

(5E/Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one → (3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one (177422-46-7) + (3S,5R)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one

Guidance literature:

With hydrogen;

DOI:10.1021/jo990445+

Reference yield: 30.0%

(5E/Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one → (5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-(5H)-furan-2-one + (3R,5S)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one (177422-46-7) + (3S,5R)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propyl)-4,5-dihydro-(3H)-furan-2-one

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 12h;

DOI:10.1021/jo960042z

upstream raw materials:

(5E)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

(5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

2,3,5,6,7-penta-O-benzoyl-D-glycero-D-gulo-heptono-1,4-lactone

Downstream raw materials:

(3R,5S)-5-[(S)-3-(tert-Butyl-diphenyl-silanyloxy)-2-hydroxy-propyl]-3-hydroxy-dihydro-furan-2-one

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