(5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

Base Information

Chemical Name:(5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one
CAS No.:177568-34-2
Molecular Formula:C₂₈H₂₀O₈
Molecular Weight:484.462
Hs Code.:

Synonyms:(5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

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Technology Process of (5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

There total 1 articles about (5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 10279-92-2
2,3,5,6,7-penta-O-benzoyl-D-glycero-D-gulo-heptono-1,4-lactone

: 177568-33-1
(5E)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

: 177568-34-2
(5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

Guidance literature:: With triethylamine; In chloroform; for 0.75h; Ambient temperature;
DOI:10.1021/jo960042z

Reference yield:

: 177568-34-2
(5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

: C₄₂H₃₆O₁₀

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C / ethyl acetate / 12 h

2: 98 percent / NaOMe / methanol / 2 h / Ambient temperature

3: 99 percent / NaBH₄ / methanol / 2 h / Ambient temperature

4: pyridine / 2 h / Ambient temperature

With pyridine; sodium tetrahydroborate; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jo960042z

Reference yield:

: 177568-34-2
(5Z)-3-(benzoyloxy)-5-((2'S)-2',3'-bis(benzoyloxy)propylidene)-(5H)-furan-2-one

: (2R,4R,6S)-7-(tert-Butyl-diphenyl-silanyloxy)-heptane-1,2,4,6-tetraol

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C / ethyl acetate / 12 h

2: 98 percent / NaOMe / methanol / 2 h / Ambient temperature

3: 60 percent / imidazole / dimethylformamide / 10 h / Ambient temperature

4: 50 percent / NaBH₄ / methanol / 4 h / Ambient temperature

With 1H-imidazole; sodium tetrahydroborate; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo960042z