3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide

Base Information

Chemical Name:3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide
CAS No.:1400277-86-2
Molecular Formula:C₂₀H₁₇N₅OS
Molecular Weight:375.454
Hs Code.:

Synonyms:3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide

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Technology Process of 3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide

There total 3 articles about 3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1400277-85-1
C₂₀H₁₇N₃O₂S₂

: 1400277-86-2
3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Reflux;
DOI:10.1080/00397911.2011.591036

Reference yield:

: 87273-75-4
3‐oxo‐N‐(4‐phenylthiazol‐2yl)butanamide

: 1400277-86-2
3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h

1.2: 24 h

2.1: hydrazine hydrate / ethanol / 6 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2011.591036

Reference yield:

: 2010-06-2
2-Amino-4-phenylthiazole

: 1400277-86-2
3-methyl-5-(phenylamino)-N-(4-phenylthiazol-2-yl)-1H-pyrazole-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: neat (no solvent) / 150 °C

2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h

2.2: 24 h

3.1: hydrazine hydrate / ethanol / 6 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2011.591036