2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol

Base Information

Chemical Name:2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol
CAS No.:1609980-41-7
Molecular Formula:C₁₇H₂₁N₅O₂
Molecular Weight:327.386
Hs Code.:

Synonyms:2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol

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Chemical Property of 2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol

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Technology Process of 2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol

There total 3 articles about 2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: (5,7-dimethyl-1,2,4-triazolo[1,5-a]pyrimidine-2-sulfonyl)methane

: 120-07-0
2,2'-(phenylimino)bis[ethanol]

: 1609980-41-7
2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol

Guidance literature:: 2,2'-(phenylimino)bis[ethanol]; With sodium hydride; In tetrahydrofuran; mineral oil; for 0.166667h; Inert atmosphere;

(5,7-dimethyl-1,2,4-triazolo[1,5-a]pyrimidine-2-sulfonyl)methane; In tetrahydrofuran; mineral oil; for 0.75h; Inert atmosphere;

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 1609980-41-7
2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 15 h / 135 °C

2.1: acetic acid; sodium tungstate (VI) dihydrate; dihydrogen peroxide / water / 1.17 h / 10 - 60 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / Inert atmosphere

3.2: 0.75 h / Inert atmosphere

With sodium tungstate (VI) dihydrate; dihydrogen peroxide; sodium hydride; acetic acid; In tetrahydrofuran; water; mineral oil;

Reference yield:

: 51646-19-6
5,7-dimethyl-2-methylthio-1,2,4-triazolo<1,5-a>pyrimidine

: 1609980-41-7
2-{[2-({5,7-dimethyl[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; sodium tungstate (VI) dihydrate; dihydrogen peroxide / water / 1.17 h / 10 - 60 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / Inert atmosphere

2.2: 0.75 h / Inert atmosphere

With sodium tungstate (VI) dihydrate; dihydrogen peroxide; sodium hydride; acetic acid; In tetrahydrofuran; water; mineral oil;