(S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide

Base Information

Chemical Name:(S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide
CAS No.:1315318-11-6
Molecular Formula:C₂₀H₂₇NO₂S
Molecular Weight:345.506
Hs Code.:

Synonyms:(S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide

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Chemical Property of (S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide

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Technology Process of (S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide

There total 6 articles about (S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1631179-23-1
1,3-dioxoisoindolin-2-yl isobutyrate

: (S)-(+)-N-(p-methoxybenzylidene)-2,4,6-trimethylphenylsulfinamide

: 1315318-11-6
(S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide

Guidance literature:: With tris[2-phenylpyridinato-C₂,N]iridium(III); diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 20 ℃; for 37h; diastereoselective reaction; Sealed tube; Inert atmosphere; Irradiation;
DOI:10.1039/c7cc03724d

Reference yield:

: C₂₅H₂₉NO₄S₂

: 1315318-11-6
(S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hexamethyldisilazane / 2-methyltetrahydrofuran; diethyl ether; toluene / -78 - 20 °C / Inert atmosphere

2: 2-methyltetrahydrofuran; diethyl ether; toluene / 20 °C / Inert atmosphere

3: 2-methyltetrahydrofuran; diethyl ether; toluene / -78 - 20 °C / Inert atmosphere

With lithium hexamethyldisilazane; In 2-methyltetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/jo201849j

Reference yield:

: 2633-66-1
2-mesitylmagnesium bromide

: 1315318-11-6
(S)-N-((S)-1-(4-methoxyphenyl)-2-methylpropyl)-2,4,6-trimethylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 4 steps

1: 2-methyltetrahydrofuran; diethyl ether / -78 °C / Inert atmosphere

2: lithium hexamethyldisilazane / 2-methyltetrahydrofuran; diethyl ether; toluene / -78 - 20 °C / Inert atmosphere

3: 2-methyltetrahydrofuran; diethyl ether; toluene / 20 °C / Inert atmosphere

4: 2-methyltetrahydrofuran; diethyl ether; toluene / -78 - 20 °C / Inert atmosphere

With lithium hexamethyldisilazane; In 2-methyltetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/jo201849j