Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol

Base Information

Chemical Name:Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol
CAS No.:909036-71-1
Molecular Formula:C₅₃H₄₂O₄
Molecular Weight:742.914
Hs Code.:

Synonyms:Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol

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Chemical Property of Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol

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Technology Process of Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol

There total 1 articles about Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21154-13-2,60077-28-3,70561-17-0
trans-(4R,5R)-1,3-dioxolane-4,5-dicarboxylic acid diethyl ester

: 3315-91-1
4-biphenylylmagnesium bromide

: 909036-71-1
Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol

Guidance literature:: In tetrahydrofuran;
DOI:10.1002/adsc.200505167

Reference yield:

: 909036-71-1
Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol

: (3aR,8aR)-4,4,8,8-Tetrakis-biphenyl-4-yl-tetrahydro-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepine 6-oxide

Guidance literature:: Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol; With triethylamine; phosphorus trichloride; In tetrahydrofuran; at 0 ℃; for 1h;

With triethylamine; In tetrahydrofuran; water;
DOI:10.1002/adsc.200505167

Reference yield:

: 909036-71-1
Bis-biphenyl-4-yl-[(4R,5R)-5-(bis-biphenyl-4-yl-hydroxy-methyl)-[1,3]dioxolan-4-yl]-methanol

: (3aR,8aR)-4,4,8,8-Tetrakis-biphenyl-4-yl-6-oxo-tetrahydro-6λ⁵-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: PCl₃; Et₃N / tetrahydrofuran / 1 h / 0 °C

1.2: Et₃N / H₂O; tetrahydrofuran

2.1: I₂ / pyridine; H₂O / 0.33 h / 20 °C

With iodine; triethylamine; phosphorus trichloride; In tetrahydrofuran; pyridine; water;
DOI:10.1002/adsc.200505167