3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose

Base Information

Chemical Name:3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose
CAS No.:126378-36-7
Molecular Formula:C₁₆H₂₁NO₅
Molecular Weight:307.346
Hs Code.:

Synonyms:3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose

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Chemical Property of 3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose

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Technology Process of 3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose

There total 1 articles about 3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-94-9
4-methoxy-aniline

: 18968-51-9,43138-66-5,63522-21-4,816444-37-8
1,2-O-isopropylidene-3-O-methyl-α-D-xylo-pentodialdo-1,4-furanose

: 126378-36-7
3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose

Guidance literature:: for 0.166667h; under 0.00030003 Torr; Neat (no solvent);
DOI:10.1021/jo200908b

Reference yield:

: 61550-02-5
(furan-2-yloxy)-trimethylsilane

: 126378-36-7
3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose

: 126378-37-8
(S)-5-[(R)-((3aR,5R,6S,6aR)-6-Methoxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-(4-methoxy-phenylamino)-methyl]-5H-furan-2-one

: 126378-38-9
(R)-5-[(R)-((3aR,5R,6S,6aR)-6-Methoxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-(4-methoxy-phenylamino)-methyl]-5H-furan-2-one

Guidance literature:: With boron trifluoride diethyl etherate; citric acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, -80 deg C, 2.) CH₃OH;
DOI:10.1021/jo00296a001

Reference yield:

: 563-70-2
bromonitromethane

: 126378-36-7
3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose

: (5S)-3-O-methyl-5,6-dideoxy-1,2-O-isopropylidene-5-p-methoxyphenylamino-6-nitro-α-D-glucofuranose

: 1357911-93-3
3-O-methyl-5,6-dideoxy-1,2-O-isopropylidene-5-p-methoxyphenylamino-6-nitro-α-D-glucofuranose

Guidance literature:: bromonitromethane; 3-O-methyl-5-deoxy-1,2-O-isopropylidene-5[(4-methoxyphenyl)imino]-α-D-xylofuranose; With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 5h;

With hydrogenchloride; In tetrahydrofuran; water; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tet.2011.12.061