{(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}B(C₆H₅)4

Base Information

• Chemical Name: {(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}B(C₆H₅)4
• CAS No.: 137436-59-0
• Molecular Formula: C₂₄H₂₀B*C₂₆H₃₉P₂Ru
• Molecular Weight: 833.847

Synonyms:{(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}B(C₆H₅)4

Chemical Property of {(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}B(C₆H₅)4

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Technology Process of {(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}B(C₆H₅)4

There total 1 articles about {(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(C₅(CH₃)5)Ru(H)2(P(CH₃)2(C₆H₅))2}B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

pentamethylcyclopentadienylruthenium dichloride (96503-27-4) + sodium tetraphenyl borate (143-66-8) + Dimethyl(phenyl)phosphine (672-66-2) → {(C5(CH3)5)Ru(H)2(P(CH3)2(C6H5))2}(1+)*B(C6H5)4(1-)={(C5(CH3)5)Ru(H)2(P(CH3)2(C6H5))2}B(C6H5)4 (137436-59-0)

Guidance literature:

With Zn; NaOCH₃; HBF₄*Et₂O; In benzene; stirring a mixt. of (C5Me5)RuCl2, Zn and PMe2Ph in benzene (overnight) under Ar or H2, addn. of NaOMe and EtOH, refluxing (5 h), evapn., extg. (benzene), evapn., redissolving in Et2O, titrn. with HBF4*Et2O, evapn., redissolving in MeOH, addn. of NaBPh4; filtration of the ppt., washing (MeOH), drying (vac.); elem. anal.;

Reference yield: 54.0%

{(C5(CH3)5)Ru(H)2(P(CH3)2(C6H5))2}(1+)*B(C6H5)4(1-)={(C5(CH3)5)Ru(H)2(P(CH3)2(C6H5))2}B(C6H5)4 (137436-59-0) → (C5(CH3)5)RuH(P(CH3)2(C6H5))2 (137436-51-2)

Guidance literature:

With NaO(t-Bu); In tetrahydrofuran; stirring a mixt. of ((C5Me5)Ru(H2)(PMe2Ph)2)BPh4 and NaO(t-Bu) in THF under Ar or H2 (overnight, room temp.); evapn., extg. (benzene), evapn., drying (vac.);

upstream raw materials:

pentamethylcyclopentadienylruthenium dichloride

sodium tetraphenyl borate

Dimethyl(phenyl)phosphine

Downstream raw materials:

(C₅(CH₃)5)RuH(P(CH₃)2(C₆H₅))2

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