((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene

Base Information

Chemical Name:((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene
CAS No.:900149-88-4
Molecular Formula:C₃₂H₆₂O₅Si₂
Molecular Weight:583.012
Hs Code.:

Synonyms:((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene

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Chemical Property of ((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene

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Technology Process of ((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene

There total 6 articles about ((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 900149-81-7
(2S,3S)-4-Benzyloxy-1-methoxymethoxy-2-methyl-butane-2,3-diol

: 13154-24-0
triisopropylsilyl chloride

: 900149-88-4
((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 24h;
DOI:10.1016/j.tet.2006.03.066

Reference yield:

: 900149-79-3
Acetic acid (E)-4-methoxymethoxy-3-methyl-but-2-enyl ester

: 900149-88-4
((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / LiOH*H₂O / tetrahydrofuran; H₂O / 12 h / 20 °C

2: 90 percent / sodium hydride; tetrabutylammonium iodide / tetrahydrofuran; various solvent(s) / 15 h / 20 °C

3: 99 percent / AD-mix-α; K2OsO4*2H2O; methanesulfonamide / (DHQ)2-PHAL; K3Fe(CN)6 / H2O; 2-methyl-propan-2-ol / 20 h / 0 °C

4: 96 percent / sodium hydride / various solvent(s); tetrahydrofuran / 24 h

With lithium hydroxide; potassium osmate(VI); AD-mix-α; methanesulfonamide; tetra-(n-butyl)ammonium iodide; sodium hydride; (DHQ)2-PHAL; potassium hexacyanoferrate(III); In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2006.03.066

Reference yield:

: 900149-80-6
((E)-4-Methoxymethoxy-3-methyl-but-2-enyloxymethyl)-benzene

: 900149-88-4
((2S,3S)-4-Methoxymethoxy-3-methyl-2,3-bis-triisopropylsilanyloxy-butoxymethyl)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / AD-mix-α; K2OsO4*2H2O; methanesulfonamide / (DHQ)2-PHAL; K3Fe(CN)6 / H2O; 2-methyl-propan-2-ol / 20 h / 0 °C

2: 96 percent / sodium hydride / various solvent(s); tetrahydrofuran / 24 h

With potassium osmate(VI); AD-mix-α; methanesulfonamide; sodium hydride; (DHQ)2-PHAL; potassium hexacyanoferrate(III); In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2006.03.066