2-hydroxyphenyl-3-oxobutanoate

Base Information

• Chemical Name: 2-hydroxyphenyl-3-oxobutanoate
• CAS No.: 57322-56-2
• Molecular Formula: C₁₀H₁₀O₄
• Molecular Weight: 194.187
• Mol file: 57322-56-2.mol

Synonyms:2-hydroxyphenyl-3-oxobutanoate

Chemical Property of 2-hydroxyphenyl-3-oxobutanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-hydroxyphenyl-3-oxobutanoate

There total 3 articles about 2-hydroxyphenyl-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

catechol bis-bromoacetate → 2-hydroxyphenyl-3-oxobutanoate (57322-56-2)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran; at -78 ℃;

DOI:10.1016/0040-4039(95)02299-6

Reference yield:

Catecholacetatmalonat (57322-55-1) → 2-hydroxyphenyl-3-oxobutanoate (57322-56-2)

Guidance literature:

With isopropylmagnesium bromide; In tetrahydrofuran;

DOI:10.1021/ja00854a074

Reference yield:

2-acetoxyphenol (2848-25-1) → 2-hydroxyphenyl-3-oxobutanoate (57322-56-2)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: iPrMgBr / tetrahydrofuran

With isopropylmagnesium bromide; In tetrahydrofuran; diethyl ether;

DOI:10.1021/ja00854a074

upstream raw materials:

Catecholacetatmalonat

2-acetoxyphenol