3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione

Base Information

• Chemical Name: 3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione
• CAS No.: 1448808-29-4
• Molecular Formula: C₁₄H₁₆N₄O₂
• Molecular Weight: 272.307

Synonyms:3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione

Chemical Property of 3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione

Chemical Property:

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Technology Process of 3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione

There total 2 articles about 3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylacetaldehyde (122-78-1) + 3-methyl-6-(1-methylhydrazinyl)pyrimidine-2,4(1H,3H)-dione (42747-84-2) → 3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione (1448808-29-4)

Guidance literature:

In ethanol; at 50 ℃; for 0.166667h; Microwave irradiation;

DOI:10.1021/jm400568p

Reference yield:

3-methyl-6-chlorouracil (4318-56-3) → 3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione (1448808-29-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 0.17 h / 100 °C / Microwave irradiation

2: ethanol / 0.17 h / 50 °C / Microwave irradiation

In ethanol;

DOI:10.1021/jm400568p

Reference yield: 38.0%

3-methyl-6-[methyl-[(E)-2-phenylethylideneamino]amino]-1Hpyrimidine-2,4-dione (1448808-29-4) → 3-benzyl-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione (878419-53-5)

Guidance literature:

With acetic acid; sodium nitrite; In water; at 0 ℃; for 6h;

DOI:10.1016/j.bmc.2019.115128

upstream raw materials:

phenylacetaldehyde

3-methyl-6-(1-methylhydrazinyl)pyrimidine-2,4(1H,3H)-dione

3-methyl-6-chlorouracil

Downstream raw materials:

3-benzyl-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione

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