C₃₈H₄₀N₆

Base Information

• Chemical Name: C₃₈H₄₀N₆
• CAS No.: 1029002-31-0
• Molecular Formula: C₃₈H₄₀N₆
• Molecular Weight: 580.776
• Mol file: 1029002-31-0.mol

Synonyms:C₃₈H₄₀N₆

Chemical Property of C₃₈H₄₀N₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₃₈H₄₀N₆

There total 3 articles about C₃₈H₄₀N₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C44H56N6Si2 (1029002-29-6) → C38H40N6 (1029002-31-0)

Guidance literature:

With potassium fluoride; In tetrahydrofuran; at 20 ℃; for 8h;

DOI:10.1002/anie.200704717

Reference yield: 62.0%

3,5-diazido-1-(tert-butyl)benzene (1029002-25-2) + 1-(tert-butyl)-3,5-diethynylbenzene (524728-78-7) → C38H40N6 (1029002-31-0)

Guidance literature:

With copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 70 ℃; for 2.33333h; Inert atmosphere;

DOI:10.1002/chem.201002340

Reference yield:

1-(tert-butyl)-3,5-diiodobenzene (148209-54-5) → C38H40N6 (1029002-31-0)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(l) iodide; sodium azide; N,N`-dimethylethylenediamine / ethanol; water / 2 h / 60 °C

2: copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 2.33 h / 70 °C / Inert atmosphere

With copper(l) iodide; sodium azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N`-dimethylethylenediamine; In ethanol; water; toluene;

DOI:10.1002/chem.201002340

upstream raw materials:

C₄₄H₅₆N₆Si₂

3,5-diazido-1-(tert-butyl)benzene

1-(tert-butyl)-3,5-diethynylbenzene

1-(tert-butyl)-3,5-diiodobenzene

Downstream raw materials:

C₅₀H₅₀N₁₂