N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide

Base Information

Chemical Name:N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide
CAS No.:1353767-31-3
Molecular Formula:C₂₄H₃₂N₂O₂
Molecular Weight:380.53
Hs Code.:

Synonyms:N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide

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Chemical Property of N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide

Chemical Property:

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Technology Process of N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide

There total 5 articles about N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 588-96-5
4-bromoethoxybenzene

: 1353776-67-6
N-[1-methyl-2-(4-piperidin-4-yl-phenyl)-ethyl]-acetamide

: 1353767-31-3
N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide

Guidance literature:: With sodium pivalate; XPhos; palladium diacetate; In toluene; tert-butyl alcohol; at 150 ℃; for 0.166667h; Microwave irradiation; Sealed tube;

Reference yield:

: 1353776-65-4
4-[4-(2-Acetylamino-propyl)-phenyl]-3,6-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester

: 1353767-31-3
N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 7 h / 20 °C / 2585.81 Torr

2: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

3: sodium pivalate; XPhos / palladium diacetate / toluene; tert-butyl alcohol / 0.17 h / 150 °C / microwave irradiation in a sealed tube

With hydrogen; sodium pivalate; trifluoroacetic acid; XPhos; palladium 10% on activated carbon; palladium diacetate; In methanol; dichloromethane; toluene; tert-butyl alcohol;

Reference yield:

: 1353776-66-5
4-[4-(2-acetylamino-propyl)-phenyl]-piperidine-1-carboxylic acid tert-butyl ester

: 1353767-31-3
N-(2-{4-[1-(4-ethoxy-phenyl)-pireridin-4-yl]-phenyl}-1-methyl-ethyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

2: sodium pivalate; XPhos / palladium diacetate / toluene; tert-butyl alcohol / 0.17 h / 150 °C / microwave irradiation in a sealed tube

With sodium pivalate; trifluoroacetic acid; XPhos; palladium diacetate; In dichloromethane; toluene; tert-butyl alcohol;