methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside

Base Information

Chemical Name:methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside
CAS No.:226885-89-8
Molecular Formula:C₁₇H₂₅IO₆
Molecular Weight:452.286
Hs Code.:

Synonyms:methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside

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Technology Process of methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside

There total 9 articles about methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 107-30-2
chloromethyl methyl ether

: 748154-79-2
(2S,3S,5S,6S)-2-Iodomethyl-6-methoxy-5-(4-methoxy-benzyloxy)-tetrahydro-pyran-3-ol

: 226885-89-8
methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2004.05.129

Reference yield:

: 226885-88-7
methyl 3-deoxy-2-O-(4-methoxybenzyl)-α-D-arabinopyranoside

: 226885-89-8
methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / I₂; Ph₃P; Imid_. / toluene

2: 91 percent / DIPEA / CH₂Cl₂

With 1H-imidazole; iodine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2004.05.129

Reference yield:

: 226885-87-6
methyl 4,6-O-benzylidene-3-deoxy-2-O-(4-methoxybenzyl)-α-D-arabinopyranoside

: 226885-89-8
methyl 3,6-dideoxy-6-iodo-2-O-(4-methoxybenzyl)-4-O-methoxymethyl-α-D-arabinopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / AcOH; H₂O / 70 °C

2: 100 percent / I₂; Ph₃P; Imid_. / toluene

3: 91 percent / DIPEA / CH₂Cl₂

With 1H-imidazole; water; iodine; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2004.05.129