Technology Process of C35H52O6Si
There total 7 articles about C35H52O6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C29H48O7Si;
With
trifluoracetyl chloride; dmap;
In
dichloromethane;
at 20 ℃;
phenyllithium;
In
tetrahydrofuran;
at -78 ℃;
for 0.5h;
Further stages.;
DOI:10.1002/ejoc.200390109
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 86 percent / imidazole / dimethylformamide / 4 h / 20 °C
2.1: 808 mg / NaBH4 / methanol / 0.5 h / 0 °C
3.1: CF3SOCl; DMAP / CH2Cl2 / 20 °C
3.2: tetrahydrofuran / 0.5 h / -78 °C
With
1H-imidazole; trifluoracetyl chloride; dmap; sodium tetrahydroborate;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200390109
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 97 percent / Pd(dba)2*Ph3P; HCOOH; NEt3 / tetrahydrofuran / 48 h / Heating
2.1: 91 percent / OsO4; 4-methylmorpholine N-oxide / tetrahydrofuran; H2O / 120 h / 20 °C
3.1: CeCl3*7H2O; NaBH4 / methanol / 0.5 h / 0 °C
3.2: 49 percent / NaIO4 / tetrahydrofuran; H2O / 3 h / 20 °C
4.1: 86 percent / imidazole / dimethylformamide / 4 h / 20 °C
5.1: 808 mg / NaBH4 / methanol / 0.5 h / 0 °C
6.1: CF3SOCl; DMAP / CH2Cl2 / 20 °C
6.2: tetrahydrofuran / 0.5 h / -78 °C
With
1H-imidazole; trifluoracetyl chloride; dmap; sodium tetrahydroborate; osmium(VIII) oxide; formic acid; cerium(III) chloride; Pd(dba)2*Ph3P; 4-methylmorpholine N-oxide; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200390109
