Technology Process of C22H25ClN2O6
There total 6 articles about C22H25ClN2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol; lithium hydroxide; water / 12 h / 40 °C
1.2: NaOAc-HOAc buffer
2.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C
With
4-methyl-morpholine; methanol; lithium hydroxide; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: calcium hypochlorite / acetic acid; acetone / 12 h / 20 °C
2.1: methanol; sodium hydroxide; water / 12 h / 20 °C
2.2: pH 6.5
3.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C
4.1: methanol; lithium hydroxide; water / 12 h / 40 °C
4.2: NaOAc-HOAc buffer
5.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C
With
4-methyl-morpholine; methanol; lithium hydroxide; sodium hydroxide; calcium hypochlorite; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
acetic acid; N,N-dimethyl-formamide; acetone;