2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide

Base Information

Chemical Name:2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide
CAS No.:774226-75-4
Molecular Formula:C₃₀H₄₇N₃O₄
Molecular Weight:513.721
Hs Code.:

Synonyms:2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide

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Chemical Property of 2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide

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Technology Process of 2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide

There total 7 articles about 2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 596111-53-4
2R-[(N-benzyloxy-N-formylamino)methyl]-6-heptenoic acid

: 774226-71-0
N-(7-octenyl)-L-tert-leucinamide

: 774226-75-4
2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;
DOI:10.1021/jm049592c

Reference yield:

: 82223-49-2
1-amino-7-octene

: 774226-75-4
2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / triethylamine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 2 h

2: trifluoroacetic acid / CH₂Cl₂ / 2 h

3: 87 percent / triethylamine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm049592c

Reference yield:

: 13175-44-5
oct-7-en-1-ol

: 774226-75-4
2R-[(N-benzyloxy-N-formylamino)methyl]-N-{1-(7-octenylcarbamoyl)-2,2-dimethylpropyl}-6-heptenoic acid amide

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / CH₂Cl₂ / 2 h

2: aq. sodium azide / dimethylformamide / 50 °C

3: LiAlH₄ / diethyl ether

4: 93 percent / triethylamine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 2 h

5: trifluoroacetic acid / CH₂Cl₂ / 2 h

6: 87 percent / triethylamine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂

With lithium aluminium tetrahydride; sodium azide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm049592c