C₄₄H₅₀N₄O₈

Base Information

Chemical Name:C₄₄H₅₀N₄O₈
CAS No.:884871-67-4
Molecular Formula:C₄₄H₅₀N₄O₈
Molecular Weight:762.903
Hs Code.:

C<sub>44</sub>H<sub>50</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:C₄₄H₅₀N₄O₈

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Chemical Property of C₄₄H₅₀N₄O₈

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Technology Process of C₄₄H₅₀N₄O₈

There total 6 articles about C₄₄H₅₀N₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1-benzyloxymethyl-5-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl)-4-(1,1-dimethyl-prop-2-ynyl)-1H-imidazole

: 884871-65-2
C₂₂H₂₂N₂O₅

: 884871-67-4
C₄₄H₅₀N₄O₈

Guidance literature:: 1-benzyloxymethyl-5-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl)-4-(1,1-dimethyl-prop-2-ynyl)-1H-imidazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

C₂₂H₂₂N₂O₅; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h;
DOI:10.1021/jo060084f

Reference yield:

: 884871-34-5
C₁₇H₁₃ClN₂O₃

: 884871-67-4
C₄₄H₅₀N₄O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: 91 percent / (TMS)3SiH; AIBN / toluene / 100 °C

2.1: 91 percent / DMAP; triethylamine / CH₂Cl₂ / 1 h / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C

3.2: 92 percent / tetrahydrofuran; hexane / 1.5 h / -78 °C

With dmap; n-butyllithium; 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; triethylamine; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/jo060084f

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 884871-67-4
C₄₄H₅₀N₄O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: 80 percent / acetic acid / ethanol / 1 h / Heating

2.1: 90 percent / triethylamine / CH₂Cl₂ / 20 °C

3.1: 91 percent / (TMS)3SiH; AIBN / toluene / 100 °C

4.1: 91 percent / DMAP; triethylamine / CH₂Cl₂ / 1 h / 20 °C

5.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C

5.2: 92 percent / tetrahydrofuran; hexane / 1.5 h / -78 °C

With dmap; n-butyllithium; 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; acetic acid; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane; toluene;
DOI:10.1021/jo060084f