Diethylamine phosphate

Base Information

• Chemical Name: Diethylamine phosphate
• CAS No.: 68109-72-8
• Molecular Formula: C4H14NO4P
• Molecular Weight: 171.133
• European Community (EC) Number: 268-485-3,262-088-9
• DSSTox Substance ID: DTXSID6071089
• Mol file: 68109-72-8.mol

Synonyms:Diethylamine phosphate;68109-72-8;Diethylammonium dihydrogen phosphate;Diethylammonium phosphate;Ethanamine, N-ethyl-, phosphate (1:1);60159-97-9;Diethylaminephosphate;N-ethylethanamine;phosphoric acid;EINECS 262-088-9;EINECS 268-485-3;N-ethylethanamine phosphate;Diethyl amine phosphate;C4H11N.xH3O4P;SCHEMBL320756;DTXSID6071089;C4-H11-N.x-H3-O4-P;DIETHYLAMINE;PHOSPHORIC ACID;AKOS015915769;FT-0624874

Chemical Property of Diethylamine phosphate

Chemical Property:

• Vapor Pressure: 5.74E-06mmHg at 25°C
• Melting Point: 153-156 °C(lit.)
• Boiling Point: 354.1 °C at 760 mmHg
• Flash Point: 168 °C
• PSA: 99.60000
• LogP: 0.07810
• Storage Temp.: Hygroscopic, Refrigerator, under inert atmosphere
• Solubility.: DMSO, Methanol, Water
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 171.06604493
• Heavy Atom Count: 10
• Complexity: 60.9

Purity/Quality:

99% ^*data from raw suppliers

DiethylammoniumDihydrogenPhosphate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

Useful:

• Canonical SMILES: CCNCC.OP(=O)(O)O
• Uses: Diethylammonium Dihydrogen Phosphate (cas# 68109-72-8) is a compound useful in organic synthesis.

Technology Process of Diethylamine phosphate

There total 2 articles about Diethylamine phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

triethylamine (121-44-8) → diethylammonium dihydrogen phosphate (68109-72-8)

Guidance literature:

With phosphoric acid; at 60 - 70 ℃; for 2h;

DOI:10.1134/S096554411302014X

Reference yield:

diethylamine (109-89-7) → diethylammonium dihydrogen phosphate (68109-72-8)

Guidance literature:

With phosphoric acid; In water; at 60 - 70 ℃;

DOI:10.1039/c4ra15590d

upstream raw materials:

triethylamine

diethylamine

Refernces

• 1、 Malla, Ali Mohammed,Parveen, Mehtab,Ahmad, Faheem,Azaz, Shaista,Alam, Mahboob. "[HSO4]-catalyzed eco-friendly and expeditious synthesis of thiazolidine and oxazolidine derivatives". . p. 19552 - 19569. Retrieved 2015/06/01.