methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate

Base Information

Chemical Name:methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate
CAS No.:146827-64-7
Molecular Formula:C₂₄H₂₉NO₆S
Molecular Weight:459.563
Hs Code.:

Synonyms:methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate

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Chemical Property of methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate

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Technology Process of methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate

There total 5 articles about methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 146827-62-5
methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>thio>propionate

: 146827-64-7
methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate

Guidance literature:: With Oxone; In methanol; water; for 14h;
DOI:10.1021/jm00056a006

Reference yield:

: 95798-23-5
1-(benzyloxycarbonyl)-4-hydroxypiperidine

: 146827-64-7
methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triphenylphosphine, diethyl azodicarboxylate (DEAD) / 1.) THF, -78 deg C, 7 min, 2.) THF, a) -78 deg C, 1 h, b) RT, 20 h

2: 1.) sodium bis(trimethylsilyl)amide / 1.) MeOH, THF, 45 min, 2.) MeOH, THF, 45 min

3: 97 percent / oxone / methanol; H₂O / 14 h

With Oxone; sodium hexamethyldisilazane; triphenylphosphine; diethylazodicarboxylate; In methanol; water;
DOI:10.1021/jm00056a006

Reference yield:

: 5669-19-2
2-Benzyl-2-propenoic acid

: 146827-64-7
methyl 2-benzyl-3-<<1-(benzyloxycarbonyl)piperidin-4-yl>sulfonyl>propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / BF₃*Et₂O / 14 h / Heating

2: 1.) sodium bis(trimethylsilyl)amide / 1.) MeOH, THF, 45 min, 2.) MeOH, THF, 45 min

3: 97 percent / oxone / methanol; H₂O / 14 h

With Oxone; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; In methanol; water;
DOI:10.1021/jm00056a006