2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone

Base Information

• Chemical Name: 2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone
• CAS No.: 1330776-66-3
• Molecular Formula: C₂₃H₂₂Cl₂O₃
• Molecular Weight: 417.332

Synonyms:2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone

Chemical Property of 2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone

Chemical Property:

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Technology Process of 2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone

There total 1 articles about 2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1,3-bis(4-chlorophenyl)prop-2-en-1-one (20725-25-1,22966-30-9,19672-59-4) + dimedone (126-81-8) → 2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone (1330776-66-3)

Guidance literature:

With cetyltrimethylammonim bromide; In water; at 120 ℃; for 7h;

DOI:10.1002/ejoc.201100374

Reference yield: 97.0%

2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone (1330776-66-3) → 2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-2-hydroxyperoxy-5,5-dimethylcyclohexane-1,3-dione (1330776-75-4)

Guidance literature:

With air; In 1,2-dichloro-ethane; at 20 ℃; for 15h;

DOI:10.1002/ejoc.201100374

Reference yield:

2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone (1330776-66-3) + C23H26OSi (1359950-48-3) → 2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-2-hydroxy-5,5-dimethylcyclohexane-1,3-dione (1330776-84-5) + (tert-butyldiphenylsilyl)(phenyl)methanone (1359950-53-0)

Guidance literature:

With oxygen; In 1,2-dichloro-ethane; at 20 ℃; for 36h;

DOI:10.1055/s-0031-1289907

upstream raw materials:

1,3-bis(4-chlorophenyl)prop-2-en-1-one

dimedone

Downstream raw materials:

2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-2-hydroxyperoxy-5,5-dimethylcyclohexane-1,3-dione

2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-2-hydroxy-5,5-dimethylcyclohexane-1,3-dione

(tert-butyldiphenylsilyl)(phenyl)methanone

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