1-(5-hydroxy-4-methoxy-2-methylbenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydro-7-isoquinolinol

Base Information

Chemical Name:1-(5-hydroxy-4-methoxy-2-methylbenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydro-7-isoquinolinol
CAS No.:89240-88-0
Molecular Formula:C₂₀H₂₅NO₄
Molecular Weight:343.423
Hs Code.:

Synonyms:1-(5-hydroxy-4-methoxy-2-methylbenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydro-7-isoquinolinol

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Chemical Property of 1-(5-hydroxy-4-methoxy-2-methylbenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydro-7-isoquinolinol

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Technology Process of 1-(5-hydroxy-4-methoxy-2-methylbenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydro-7-isoquinolinol

There total 20 articles about 1-(5-hydroxy-4-methoxy-2-methylbenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydro-7-isoquinolinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 89240-94-8
(+/-)-3',7-diacetoxy-6'-methyl-4',6-dimethoxy-1,2,3,4-tetrahydro-2-ethoxycarbonyl-1-benzyl-isoquinoline

: 89240-88-0
1-(5-hydroxy-4-methoxy-2-methylbenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydro-7-isoquinolinol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 6h; Heating;

Reference yield:

: 89300-66-3
7-Acetoxy-1-(5-acetoxy-2-chloromethyl-4-methoxy-benzyl)-6-methoxy-3,4-dihydro-1H-isoquinoline-2-carboxylic acid ethyl ester

: 89240-88-0
1-(5-hydroxy-4-methoxy-2-methylbenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydro-7-isoquinolinol

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / H₂ / 10percent Pd/C / acetic acid / 21 h / 2585.7 Torr / Ambient temperature

2: 72 percent / LAH / tetrahydrofuran / 6 h / Heating

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; acetic acid;