N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide

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Chemical Name:N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide
CAS No.:1395093-44-3
Molecular Formula:C₄₆H₄₉N₅
Molecular Weight:671.929
Hs Code.:

Synonyms:N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide

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Chemical Property of N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide

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Technology Process of N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide

There total 5 articles about N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24544-04-5
2,6-diisopropylbenzenamine

: 1395093-43-2
9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carbonitrile

: 1395093-44-3
N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide

Guidance literature:: 2,6-diisopropylbenzenamine; With trimethylaluminum; In toluene; at 0 - 20 ℃; for 2.75h;

9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carbonitrile; In toluene; at 90 ℃; for 60h;

Reference yield:

: 98-80-6
phenylboronic acid

: 1395093-44-3
N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium phosphate monohydrate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; water / Reflux

2.1: triphenylphosphine / 1,2-dichloro-benzene / 24 h / Reflux

3.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / m-xylene / 132 h / Reflux

4.1: trimethylaluminum / toluene / 2.75 h / 0 - 20 °C

4.2: 60 h / 90 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; potassium phosphate monohydrate; trimethylaluminum; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; m-xylene; 1,2-dichloro-benzene; toluene;

Reference yield:

: 166263-24-7
2-nitro-(1,1'-biphenyl)-4-carbonitrile

: 1395093-44-3
N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine / 1,2-dichloro-benzene / 24 h / Reflux

2.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / m-xylene / 132 h / Reflux

3.1: trimethylaluminum / toluene / 2.75 h / 0 - 20 °C

3.2: 60 h / 90 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; trimethylaluminum; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In m-xylene; 1,2-dichloro-benzene; toluene;