2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole

Base Information

Chemical Name:2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole
CAS No.:1395093-45-4
Molecular Formula:C₄₈H₄₉N₅
Molecular Weight:695.951
Hs Code.:

Synonyms:2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole

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Chemical Property of 2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole

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Technology Process of 2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole

There total 6 articles about 2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 107-20-0
2-chloroethanal

: 1395093-44-3
N-(2,6-diisopropylphenyl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole-2-carboximidamide

: 1395093-45-4
2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole

Guidance literature:: With sodium hydrogencarbonate; In isopropyl alcohol; for 48h; Reflux;

Reference yield:

: 98-80-6
phenylboronic acid

: 1395093-45-4
2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium phosphate monohydrate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; water / Reflux

2.1: triphenylphosphine / 1,2-dichloro-benzene / 24 h / Reflux

3.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / m-xylene / 132 h / Reflux

4.1: trimethylaluminum / toluene / 2.75 h / 0 - 20 °C

4.2: 60 h / 90 °C

5.1: sodium hydrogencarbonate / isopropyl alcohol / 48 h / Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; potassium phosphate monohydrate; trimethylaluminum; sodium hydrogencarbonate; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; m-xylene; 1,2-dichloro-benzene; isopropyl alcohol; toluene;

Reference yield:

: 166263-24-7
2-nitro-(1,1'-biphenyl)-4-carbonitrile

: 1395093-45-4
2-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-9-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)phenyl)-9H-carbazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine / 1,2-dichloro-benzene / 24 h / Reflux

2.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / m-xylene / 132 h / Reflux

3.1: trimethylaluminum / toluene / 2.75 h / 0 - 20 °C

3.2: 60 h / 90 °C

4.1: sodium hydrogencarbonate / isopropyl alcohol / 48 h / Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; trimethylaluminum; sodium hydrogencarbonate; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In m-xylene; 1,2-dichloro-benzene; isopropyl alcohol; toluene;