S-octyl diphenylphosphinothioate

Base Information

• Chemical Name: S-octyl diphenylphosphinothioate
• CAS No.: 102462-49-7
• Molecular Formula: C₂₀H₂₇OPS
• Molecular Weight: 346.474
• Mol file: 102462-49-7.mol

Synonyms:S-octyl diphenylphosphinothioate

Chemical Property of S-octyl diphenylphosphinothioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-octyl diphenylphosphinothioate

There total 9 articles about S-octyl diphenylphosphinothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Octanethiol (111-88-6) + Diphenylphosphine oxide (4559-70-0) → S-octyl diphenylphosphinothioate (102462-49-7)

Guidance literature:

With tert-Butyl peroxybenzoate; potassium iodide; In dimethyl sulfoxide; at 20 ℃; for 4h;

DOI:10.1039/c4gc00944d

Reference yield: 88.0%

N-(1-octylthio)succinimide + Diphenylphosphine oxide (4559-70-0) → S-octyl diphenylphosphinothioate (102462-49-7)

Guidance literature:

In neat (no solvent); at 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2019.150965

Reference yield: 87.0%

diphenyl-phosphinothioic acid S-pent-4-ynyl ester (934538-84-8) + oct-1-ene (111-66-0,25068-25-1) → S-octyl diphenylphosphinothioate (102462-49-7)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); thiophenol; In toluene; for 1h; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2008.08.108

upstream raw materials:

dioctyl disulfide

1,1,2,2-tetraphenyldiphosphane-1,2-dioxide

diphenyl-phosphinothioic acid S-pent-4-ynyl ester

oct-1-ene