pentamethyl-6-(triphenylgermyl)borazine

Base Information

Chemical Name:pentamethyl-6-(triphenylgermyl)borazine
CAS No.:22871-78-9
Molecular Formula:C₂₃H₃₀B₃GeN₃
Molecular Weight:453.534
Hs Code.:

Synonyms:pentamethyl-6-(triphenylgermyl)borazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentamethyl-6-(triphenylgermyl)borazine

Chemical Property:

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Technology Process of pentamethyl-6-(triphenylgermyl)borazine

There total 4 articles about pentamethyl-6-(triphenylgermyl)borazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 13058-05-4
6-chloro-1,2,3,4,5-pentamethylborazine

: 57482-41-4
Triphenylgermyl-kalium

: 22871-78-9
pentamethyl-6-(triphenylgermyl)borazine

Guidance literature:: In tetrahydrofuran; equiv. mol amt.; 20°C;
DOI:10.1016/S0022-328X(00)88617-9

Reference yield: 71.0%

: 351345-73-8
triphenylgermyllithium-diethylether(1/3)

: 21130-45-0
1,2,3,4,5-pentamethyl-6-bromoborazine

: 22871-78-9
pentamethyl-6-(triphenylgermyl)borazine

Guidance literature:: In diethyl ether; hexane; byproducts: LiBr; all manipulations under N2 or Ar; equimolar amts. of starting compds., freshly prepd. soln. of Ge compd. in Et2O cooled to -78°C, treatedwith soln. of borazine derivative in hexane, stirred for 1 h at ambient temp.; all volatiles evapd. in vac., residue treated with hexane, filtered, filtrate cooled to -30°C, allowed to stand for several d; elem. anal.;
DOI:10.1002/1521-3749(200105)627:5<1003::AID-ZAAC1003>3.0.CO;2-E

Reference yield:

: 2816-43-5
triphenylgermane

: 22871-78-9
pentamethyl-6-(triphenylgermyl)borazine

Guidance literature:: Multi-step reaction with 2 steps

1: hexane; diethyl ether

2: hexane; diethyl ether

In diethyl ether; hexane;
DOI:10.1002/1521-3749(200105)627:5<1003::AID-ZAAC1003>3.0.CO;2-E