Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose

Base Information

Chemical Name:Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose
CAS No.:83434-58-6
Molecular Formula:C₂₃H₂₂O₉
Molecular Weight:442.422
Hs Code.:

Synonyms:Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose

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Chemical Property of Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose

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Technology Process of Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose

There total 4 articles about Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6893-67-0
1,2-O-isopropylidene-3,5-di-O-benzoyl-α-D-xylofuranose

: 108-24-7
acetic anhydride

: 95530-07-7
1,2-di-O-acetyl-3,5-di-O-benzoyl-β-D-xylofuranose

: 83434-58-6
Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose

Guidance literature:: With sulfuric acid; acetic acid; Yield given; 0 deg C - room temp., 12.5 h;

Reference yield:

: 20881-04-3
1,2:3,5-di-O-isopropylidene-D-xylofuranose

: 83434-58-6
Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / water / 24 h / 20 °C

2: pyridine / dichloromethane / 44 h / 0 - 20 °C

3: sulfuric acid / acetic acid / 40 h / 20 °C

With pyridine; sulfuric acid; acetic acid; In dichloromethane; water; acetic acid;
DOI:10.1016/j.tet.2014.02.035

Reference yield:

: 20031-21-4
1,2-O-isopropylidene-α-D-xylose

: 83434-58-6
Di-O-benzoyl-3,5 di-O-acetyl-1,2 α-D-xylofurannose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 44 h / 0 - 20 °C

2: sulfuric acid / acetic acid / 40 h / 20 °C

With pyridine; sulfuric acid; In dichloromethane; acetic acid;
DOI:10.1016/j.tet.2014.02.035