3,4,5-trimethoxyaniline hydrochloride

Base Information

• Chemical Name: 3,4,5-trimethoxyaniline hydrochloride
• CAS No.: 102439-00-9
• Molecular Formula: C₉H₁₃NO₃*ClH
• Molecular Weight: 219.668
• Mol file: 102439-00-9.mol

Synonyms:3,4,5-trimethoxyaniline hydrochloride

Chemical Property of 3,4,5-trimethoxyaniline hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4,5-trimethoxyaniline hydrochloride

There total 3 articles about 3,4,5-trimethoxyaniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5-Trimethoxyaniline (24313-88-0) → 3,4,5-trimethoxyaniline hydrochloride (102439-00-9)

Guidance literature:

With hydrogenchloride; In diethyl ether;

Reference yield:

1,2,3-trimethoxybenzene (634-36-6) → 3,4,5-trimethoxyaniline hydrochloride (102439-00-9)

Guidance literature:

Multi-step reaction with 2 steps

1: nitric acid; silica gel / dichloromethane / 20 °C

2: tin(ll) chloride; hydrogenchloride / ethanol; water / Reflux

With hydrogenchloride; nitric acid; silica gel; tin(ll) chloride; In ethanol; dichloromethane; water;

DOI:10.1002/pola.28990

Reference yield:

3,4,5-trimethoxy-1-nitrobenzene (6307-90-0) → 3,4,5-trimethoxyaniline hydrochloride (102439-00-9)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In ethanol; water; Reflux;

DOI:10.1002/pola.28990

upstream raw materials:

3,4,5-Trimethoxyaniline

1,2,3-trimethoxybenzene

3,4,5-trimethoxy-1-nitrobenzene

Downstream raw materials:

methyl 6-amino-2,3,4-trimethoxy benzoate

6-amino-2,3,4-trimethoxybenzoic acid

1-(3,4,5-trimethoxyphenyl)thiourea

(3,4,5-trimethoxyphenyl)isothiocyanate