C₄₄H₂₆N₄NiO

Base Information

• Chemical Name: C₄₄H₂₆N₄NiO
• CAS No.: 1095581-07-9
• Molecular Formula: C₄₄H₂₆N₄NiO
• Molecular Weight: 685.407
• Mol file: 1095581-07-9.mol

Synonyms:C₄₄H₂₆N₄NiO

Chemical Property of C₄₄H₂₆N₄NiO

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₄₄H₂₆N₄NiO

There total 7 articles about C₄₄H₂₆N₄NiO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C44H26N6NiO (914916-61-3) → C44H26N4NiO (1095581-07-9)

Guidance literature:

In dichloromethane; for 9h; UV-irradiation; Inert atmosphere;

DOI:10.1021/ja800094e

Reference yield: 28.0%

Tetrahydrofurfuryl alcohol (97-99-4) + Ni(Ph4C20H6N4O(N2)) (914916-61-3) → (2-hydroxy-5,10,15,20-tetraphenylporphyrinato)nickel(II) (112803-38-0) + Ni(Ph3C26H10N4(OH)) (1095581-07-9) + Ni(Ph4C19H7N4(COOCH2THF)) (1095580-99-6)

Guidance literature:

In dichloromethane; Irradiation (UV/VIS); photolysis at 200 W and >=345 nm of diazochlorin deriv. in 1:4 mixt. of CH2Cl2 and furfurol deriv. at 10°C for 9 h;

DOI:10.1021/ja800094e

Reference yield: 28.0%

Tetrahydrofurfuryl alcohol (97-99-4) + C44H26N6NiO (914916-61-3) → C44H28N4NiO (112803-38-0) + C44H26N4NiO (1095581-07-9) + C49H36N4NiO3 (1095580-99-6)

Guidance literature:

In dichloromethane; for 9h; UV-irradiation; Inert atmosphere;

DOI:10.1021/ja800094e

upstream raw materials:

Ni(Ph₄C₂₀H₆N₄O(N₂))

butan-1-ol

Tetrahydrofurfuryl alcohol

toluene-4-sulfonic acid hydrazide