Technology Process of C26H38O6
There total 19 articles about C26H38O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 15 steps
2: 92 percent / LDA / tetrahydrofuran / 0.04 h / -78 °C
3: 75 percent / 1) LDA, 2) CF3COOH / tetrahydrofuran / -78 °C
4: 83 percent / LiAlH4 / tetrahydrofuran / -30 °C
5: 95 percent / pyridine
6: 92 percent / NaH / tetrahydrofuran
7: 1) Zn-Cu, 2) Zn, NH4Cl / 1) ether, room temperature, 5.5 h; 2) MeOH, 0 deg C
8: 74 percent / methanol / Ambient temperature
9: NaBH4 / methanol
10: 1) MsCl, pyridine; 2) t-BuOK / 2) DMSO
11: 89 percent / HgCl2 / acetonitrile; H2O / 40 °C
12: TsOH
13: PCC, MS-3A
14: CH2Cl2
15: NaBH4, NiCl2*6H2O / methanol
With
pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; potassium tert-butylate; copper; sodium hydride; ammonium chloride; toluene-4-sulfonic acid; methanesulfonyl chloride; pyridinium chlorochromate; trifluoroacetic acid; mercury dichloride; nickel dichloride; zinc; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/S0040-4039(00)82126-7
- Guidance literature:
-
Multi-step reaction with 15 steps
2: 92 percent / LDA / tetrahydrofuran / 0.04 h / -78 °C
3: 75 percent / 1) LDA, 2) CF3COOH / tetrahydrofuran / -78 °C
4: 83 percent / LiAlH4 / tetrahydrofuran / -30 °C
5: 95 percent / pyridine
6: 92 percent / NaH / tetrahydrofuran
7: 1) Zn-Cu, 2) Zn, NH4Cl / 1) ether, room temperature, 5.5 h; 2) MeOH, 0 deg C
8: 74 percent / methanol / Ambient temperature
9: NaBH4 / methanol
10: 1) MsCl, pyridine; 2) t-BuOK / 2) DMSO
11: 89 percent / HgCl2 / acetonitrile; H2O / 40 °C
12: TsOH
13: PCC, MS-3A
14: CH2Cl2
15: NaBH4, NiCl2*6H2O / methanol
With
pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; potassium tert-butylate; copper; sodium hydride; ammonium chloride; toluene-4-sulfonic acid; methanesulfonyl chloride; pyridinium chlorochromate; trifluoroacetic acid; mercury dichloride; nickel dichloride; zinc; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/S0040-4039(00)82126-7