2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose

Base Information

• Chemical Name: 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose
• CAS No.: 209671-44-3
• Molecular Formula: C₁₈H₂₇NO₉
• Molecular Weight: 401.414
• Mol file: 209671-44-3.mol

Synonyms:2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose

Chemical Property of 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose

There total 1 articles about 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-O-(β-D-galactopyranosyl)-D-arabinose (61272-23-9,130767-77-0,130767-78-1) + benzylamine (100-46-9) → 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose (209671-44-3)

Guidance literature:

In ethanol; for 1.5h; Heating;

DOI:10.1016/S0040-4020(98)00294-4

Reference yield: 79.0%

copper(I) cyanide (544-92-3) + 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose (209671-44-3) → 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-glucononitrile (72521-05-2)

Guidance literature:

With acetic acid; In ethanol; for 5h; Ambient temperature;

DOI:10.1016/S0008-6215(00)80763-6

Reference yield:

sodium cyanide (143-33-9,25596-52-5) + 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-arabinose (209671-44-3) → 2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-glucononitrile (72521-05-2)

Guidance literature:

With acetic acid; In ethanol; at 0 - 20 ℃; for 5.9h;

DOI:10.1016/S0040-4020(98)00294-4

upstream raw materials:

3-O-(β-D-galactopyranosyl)-D-arabinose

benzylamine

Downstream raw materials:

2-benzylamino-2-deoxy-3-O-(β-D-galactopyranosyl)-D-glucononitrile