1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane

Base Information

Chemical Name:1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane
CAS No.:412929-88-5
Molecular Formula:C₂₁H₃₇NO₂S
Molecular Weight:367.596
Hs Code.:

Synonyms:1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane

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Chemical Property of 1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane

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Technology Process of 1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane

There total 4 articles about 1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 100-41-4,27536-89-6
ethylbenzene

: 412929-85-2
N-tert-butyl-N-(1-tert-butyl-2-ethylsulfinyl)propyl nitroxide

: 412929-88-5
1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane

Guidance literature:: With di-tert-butyl diperoxyoxalate; In ethylbenzene; at 35 ℃; for 15h;
DOI:10.1021/ma011063k

Reference yield:

: 630-19-3
pivalaldehyde

: 412929-88-5
1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane

Guidance literature:: Multi-step reaction with 4 steps

1.1: 52 percent / p-toluene-sulfonic acid / diethyl ether / 48 h / 20 °C

2.1: n-BuLi / tetrahydrofuran / -20 °C

2.2: 66 percent / tetrahydrofuran / 4 h / -78 °C

3.1: 49 percent / Cu(OAc)2*H₂O / methanol / 2 h / 20 °C

4.1: 28 percent / di-tert-butyl peroxalate / ethylbenzene / 15 h / 35 °C

With n-butyllithium; copper diacetate; di-tert-butyl diperoxyoxalate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; ethylbenzene;
DOI:10.1021/ma011063k

Reference yield:

: 72331-68-1
N-tert-butyl-α-tert-butyl nitrone

: 412929-88-5
1-phenyl-2-{N-tert-butyl-N-[1-tert-butyl-2-(ethylsulfinyl)propyl]aminnooxy}ethane

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran / -20 °C

1.2: 66 percent / tetrahydrofuran / 4 h / -78 °C

2.1: 49 percent / Cu(OAc)2*H₂O / methanol / 2 h / 20 °C

3.1: 28 percent / di-tert-butyl peroxalate / ethylbenzene / 15 h / 35 °C

With n-butyllithium; copper diacetate; di-tert-butyl diperoxyoxalate; In tetrahydrofuran; methanol; ethylbenzene;
DOI:10.1021/ma011063k