Technology Process of 2-<2-(3,4-dimethoxyphenyl)ethyl>-3,4-dihydro-1(2H)-isoquinoline
There total 7 articles about 2-<2-(3,4-dimethoxyphenyl)ethyl>-3,4-dihydro-1(2H)-isoquinoline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
perchloric acid; hydrogen;
palladium on activated charcoal;
In
ethanol;
at 50 ℃;
for 8h;
under 1748 - 3420 Torr;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 7.52 g / K2CO3 / benzene / 4 h / Heating
2: NaBH4 / ethanol / 24 h / Ambient temperature
3: 50 percent / EDTA*2Na*2H2O, Hg(OAc)2 / acetic acid; H2O / 1.5 h / 110 °C
4: 57 percent / EDTA*2Na*2H2O, Hg(OAc)2 / acetic acid; H2O / 24 h / Heating
5: 95 percent / 70percent aq. HClO4, H2 / 10percent Pd/C / ethanol / 8 h / 50 °C / 1748 - 3420 Torr
With
sodium tetrahydroborate; perchloric acid; mercury(II) diacetate; hydrogen; edetate disodium; potassium carbonate;
palladium on activated charcoal;
In
ethanol; water; acetic acid; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 7.52 g / K2CO3 / benzene / 4 h / Heating
2: NaBH4 / ethanol / 24 h / Ambient temperature
3: 50 percent / EDTA*2Na*2H2O, Hg(OAc)2 / acetic acid; H2O / 1.5 h / 110 °C
4: 57 percent / EDTA*2Na*2H2O, Hg(OAc)2 / acetic acid; H2O / 24 h / Heating
5: 95 percent / 70percent aq. HClO4, H2 / 10percent Pd/C / ethanol / 8 h / 50 °C / 1748 - 3420 Torr
With
sodium tetrahydroborate; perchloric acid; mercury(II) diacetate; hydrogen; edetate disodium; potassium carbonate;
palladium on activated charcoal;
In
ethanol; water; acetic acid; benzene;
