C₃₃H₆₁NO₂SSi₂

Base Information

Chemical Name:C₃₃H₆₁NO₂SSi₂
CAS No.:1314868-90-0
Molecular Formula:C₃₃H₆₁NO₂SSi₂
Molecular Weight:592.09
Hs Code.:

C<sub>33</sub>H<sub>61</sub>NO<sub>2</sub>SSi<sub>2</sub>

Synonyms:C₃₃H₆₁NO₂SSi₂

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Chemical Property of C₃₃H₆₁NO₂SSi₂

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Technology Process of C₃₃H₆₁NO₂SSi₂

There total 11 articles about C₃₃H₆₁NO₂SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: Triethyl-[(1R,3aR,4S,7aR)-1-((R)-3-iodo-1-methyl-propyl)-7a-methyl-octahydro-inden-4-yloxy]-silane

: ((tert-butyldimethylsilyl)imino)(methyl)(phenyl)-λ⁶-sulfanone

: 1314868-90-0
C₃₃H₆₁NO₂SSi₂

Guidance literature:: (+)-(S)-N-tert-butyldimethylsilyl-S-methyl-S-phenylsulfoximine; With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; hexanes; at -78 ℃; for 0.5h; Inert atmosphere;

Triethyl-[(1R,3aR,4S,7aR)-1-((R)-3-iodo-1-methyl-propyl)-7a-methyl-octahydro-inden-4-yloxy]-silane; In tetrahydrofuran; hexanes; at -78 - 20 ℃; for 8h; Inert atmosphere;

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 1314868-90-0
C₃₃H₆₁NO₂SSi₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C / Inert atmosphere

2.2: 8 h / -78 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; hexanes; dichloromethane;

Reference yield:

: 300344-32-5
(8S,20S)-de-A,B-8-triethylsilyloxy-20-(iodomethyl)-pregnane

: 1314868-90-0
C₃₃H₆₁NO₂SSi₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethyl sulfoxide / 1.5 h / 70 °C

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / 0 °C

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / 0 °C

4.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 17 h / 0 - 20 °C / Inert atmosphere

5.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C / Inert atmosphere

5.2: 8 h / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; iodine; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran; hexanes; dichloromethane; dimethyl sulfoxide; toluene;