C₂₃H₃₅NO₈

Base Information

Chemical Name:C₂₃H₃₅NO₈
CAS No.:1332721-80-8
Molecular Formula:C₂₃H₃₅NO₈
Molecular Weight:453.533
Hs Code.:

C<sub>23</sub>H<sub>35</sub>NO<sub>8</sub>

Synonyms:C₂₃H₃₅NO₈

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Chemical Property of C₂₃H₃₅NO₈

Chemical Property:

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Technology Process of C₂₃H₃₅NO₈

There total 14 articles about C₂₃H₃₅NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₅NO₇

: 1332721-80-8
C₂₃H₃₅NO₈

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 0 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ol202306d

Reference yield:

: 955959-57-6
C₂₀H₂₅NO₇

: 1332721-80-8
C₂₃H₃₅NO₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 25 h / 20 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 45 h / 0 - 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 33 h / 0 - 20 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 6.5 h / -78 °C / Inert atmosphere

5.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 38 h / 0 °C / Molecular sieve; Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

7.1: Jones reagent / acetone / 0.5 h / 0 °C / Inert atmosphere

8.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 5 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium chlorite; sodium tetrahydroborate; Jones reagent; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; oxalyl dichloride; tetrabutyl ammonium fluoride; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol; 7.1: Jones oxidation / 8.1: Pinnick oxidation;
DOI:10.1021/ol202306d

Reference yield:

: 955959-40-7
(3R,3aS,4S,6aR)-methyl 4-((R)-3-(benzyloxy)-2-methylpropyl)-hexahydro-3a-hydroxy-1,3-dimethyl-2,6-dioxo-1H-furo[3,4-b]pyrrole-6a-carboxylate

: 1332721-80-8
C₂₃H₃₅NO₈

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium hydroxide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 25 h / 20 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 45 h / 0 - 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 33 h / 0 - 20 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 6.5 h / -78 °C / Inert atmosphere

6.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 38 h / 0 °C / Molecular sieve; Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

8.1: Jones reagent / acetone / 0.5 h / 0 °C / Inert atmosphere

9.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 5 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium chlorite; sodium tetrahydroborate; Jones reagent; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; oxalyl dichloride; tetrabutyl ammonium fluoride; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol; 8.1: Jones oxidation / 9.1: Pinnick oxidation;
DOI:10.1021/ol202306d