benzil mono-oxime mono-(p-nitrophenyl)hydrazone

Base Information

• Chemical Name: benzil mono-oxime mono-(p-nitrophenyl)hydrazone
• CAS No.: 132544-96-8
• Molecular Formula: C₂₀H₁₆N₄O₃
• Molecular Weight: 360.372

Synonyms:benzil mono-oxime mono-(p-nitrophenyl)hydrazone

Chemical Property of benzil mono-oxime mono-(p-nitrophenyl)hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzil mono-oxime mono-(p-nitrophenyl)hydrazone

There total 2 articles about benzil mono-oxime mono-(p-nitrophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

benzil mono(p-nitrophenylhydrazone) (4702-72-1) → benzil bis-(p-nitrophenyl)hydrazone (74741-24-5) + benzil mono-oxime mono-(p-nitrophenyl)hydrazone (132544-96-8)

Guidance literature:

With hydrogenchloride; hydroxylamine hydrochloride; In pyridine; ethanol; for 20h; Heating;

DOI:10.1002/jps.2600810615

Reference yield: 67.0%

benzilmonoxime (574-15-2,574-16-3,14090-77-8,5351-34-8) + 4-nitrophenylhydrazone (100-16-3) → benzil mono-oxime mono-(p-nitrophenyl)hydrazone (132544-96-8)

Guidance literature:

In ethanol; acetic acid; at 80 - 85 ℃; for 2h;

Reference yield: 73.0%

benzil mono-oxime mono-(p-nitrophenyl)hydrazone (132544-96-8) → 2-(p-nitrophenyl)-4,5-diphenyl-2H-1,2,3-triazole 1-oxide (112700-97-7)

Guidance literature:

With lead(IV) acetate; In dichloromethane; for 0.5h; Heating;

upstream raw materials:

benzilmonoxime

4-nitrophenylhydrazone

benzil mono(p-nitrophenylhydrazone)

Downstream raw materials:

2-(4-nitrophenyl)-4,5-diphenyl-2H-1,2,3-triazole

2-(p-nitrophenyl)-4,5-diphenyl-2H-1,2,3-triazole 1-oxide

2-(p-aminophenyl)-4,5-diphenyl-2H-1,2,3-triazole

2-(4-Nitro-phenyl)-4,6-diphenyl-2,5-dihydro-[1,2,3]triazine-5-carboxylic acid methyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 132544-96-8 benzil mono-oxime mono-(p-nitrophenyl)hydrazone

Send

Send

Metric Ton KG G Pound L ML

Send

Send