9-benzyl-9-xanthydrol

Base Information

• Chemical Name: 9-benzyl-9-xanthydrol
• CAS No.: 121005-35-4
• Molecular Formula: C₂₀H₁₆O₂
• Molecular Weight: 288.346
• Mol file: 121005-35-4.mol

Synonyms:9-benzyl-9-xanthydrol

Chemical Property of 9-benzyl-9-xanthydrol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-benzyl-9-xanthydrol

There total 3 articles about 9-benzyl-9-xanthydrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

xanth-9-one (90-47-1) + benzyl chloride (100-44-7) → 9-benzyl-9-xanthydrol (121005-35-4)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) ether, reflux, 30 min, 2.) a) reflux, 15 min;

DOI:10.1021/jo00280a026

Reference yield:

9-hydroxyxanthene (90-46-0) → 9-benzyl-9-xanthydrol (121005-35-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: iodine / dichloromethane / 0.08 h / 25 °C

2.1: iodine; magnesium / tetrahydrofuran / 1.5 h / Reflux; Inert atmosphere

2.2: 2 h / Reflux; Inert atmosphere

With iodine; magnesium; In tetrahydrofuran; dichloromethane; 2.2: |Grignard Reaction;

DOI:10.17344/acsi.2017.3841

Reference yield:

xanth-9-one (90-47-1) → 9-benzyl-9-xanthydrol (121005-35-4)

Guidance literature:

With benzene; Reaktion ueber mehrere Stufen;

upstream raw materials:

xanth-9-one

benzyl chloride

9-hydroxyxanthene

Downstream raw materials:

9-benzyl-xanthene

xanth-9-one

toluene

9-Benzylidene-9H-xanthene

Refernces

• 1、 Badejo, Ibraheem T.,Karaman, Rafik,Fry, James L.. "Unstable Compounds. Synthesis and Experimental and Computational Study of the Chemical Behavior of 9--9-xanthydrol". . p. 4591 - 4596. Retrieved 2007/10/02.