D-LUCIFERIN-6-O-BETA-D-GALACTOPYRANOSIDE

Base Information

• Chemical Name: D-LUCIFERIN-6-O-BETA-D-GALACTOPYRANOSIDE
• CAS No.: 131474-38-9
• Molecular Formula: C₁₇H₁₈N₂O₈S₂
• Molecular Weight: 442.471
• Mol file: 131474-38-9.mol

Synonyms:4-Thiazolecarboxylicacid, 2-[6-(b-D-galactopyranosyloxy)-2-benzothiazolyl]-4,5-dihydro-,(S)-; Lugal

Chemical Property of D-LUCIFERIN-6-O-BETA-D-GALACTOPYRANOSIDE

Chemical Property:

• Vapor Pressure: 3.47E-26mmHg at 25°C
• Boiling Point: 788.3°Cat760mmHg
• Flash Point: 430.6°C
• PSA: 215.47000
• Density: 1.94g/cm³
• LogP: -1.14280

Purity/Quality:

98% ^*data from raw suppliers

D-Luciferin-6-O b-D-galactopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of D-LUCIFERIN-6-O-BETA-D-GALACTOPYRANOSIDE

There total 3 articles about D-LUCIFERIN-6-O-BETA-D-GALACTOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-cyano-6-hydroxybenzothiazole (939-69-5) → 6-O-β-D-galactopyranosyl-luciferin (131474-37-8,131474-38-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / M sodium hydroxide / acetone

2: 1.) potassium carbonate, 2.) ammonia / 1.) water, methanol, chloroform, 15 min, 2.) methanol, 3 h

With sodium hydroxide; ammonia; potassium carbonate; In acetone;

DOI:10.1016/0008-6215(90)80142-P

Reference yield:

1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside (3068-32-4) → 6-O-β-D-galactopyranosyl-luciferin (131474-37-8,131474-38-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / M sodium hydroxide / acetone

2: 1.) potassium carbonate, 2.) ammonia / 1.) water, methanol, chloroform, 15 min, 2.) methanol, 3 h

With sodium hydroxide; ammonia; potassium carbonate; In acetone;

DOI:10.1016/0008-6215(90)80142-P

Reference yield:

D-cysteine hydrochloride (32443-99-5) + 2-cyano-6-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)benzothiazole (131474-32-3) → 6-O-β-D-galactopyranosyl-luciferin (131474-37-8,131474-38-9)

Guidance literature:

With ammonia; potassium carbonate; Yield given. Multistep reaction; 1.) water, methanol, chloroform, 15 min, 2.) methanol, 3 h;

DOI:10.1016/0008-6215(90)80142-P

upstream raw materials:

D-cysteine hydrochloride

2-cyano-6-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)benzothiazole

2-cyano-6-hydroxybenzothiazole

1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

Downstream raw materials:

D-Galactose

(R)-2-(6-hydroxybenzo[d]thiazol-2-yl)-4,5-dihydrothiazole-4-carboxylic acid

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