2,4,6-trimethyl-3-nitrobenzeneacetonitrile

Base Information

Chemical Name:2,4,6-trimethyl-3-nitrobenzeneacetonitrile
CAS No.:205517-05-1
Molecular Formula:C₁₁H₁₂N₂O₂
Molecular Weight:204.228
Hs Code.:

Synonyms:2,4,6-trimethyl-3-nitrobenzeneacetonitrile

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Chemical Property of 2,4,6-trimethyl-3-nitrobenzeneacetonitrile

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Technology Process of 2,4,6-trimethyl-3-nitrobenzeneacetonitrile

There total 2 articles about 2,4,6-trimethyl-3-nitrobenzeneacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 34688-71-6
mesitylacetonitrile

: 205517-05-1
2,4,6-trimethyl-3-nitrobenzeneacetonitrile

Guidance literature:: With nitric acid; at 40 ℃; for 0.0833333h;
DOI:10.1002/1522-2675(20000906)83:9<2246::AID-HLCA2246>3.0.CO;2-X

Reference yield:

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 205517-05-1
2,4,6-trimethyl-3-nitrobenzeneacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / dimethylsulfoxide / 0.5 h / 80 °C

2: 84 percent / 70 percent HNO₃; conc. H₂SO₄; AcOH / 1 h

With sulfuric acid; nitric acid; acetic acid; In dimethyl sulfoxide; 1: Substitution / 2: Nitration;
DOI:10.1021/jm9900063