methyl 3-amino-2,4,6-trimethylphenylacetate

Base Information

Chemical Name:methyl 3-amino-2,4,6-trimethylphenylacetate
CAS No.:205516-96-7
Molecular Formula:C₁₂H₁₇NO₂
Molecular Weight:207.272
Hs Code.:

Synonyms:methyl 3-amino-2,4,6-trimethylphenylacetate

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Chemical Property of methyl 3-amino-2,4,6-trimethylphenylacetate

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Technology Process of methyl 3-amino-2,4,6-trimethylphenylacetate

There total 4 articles about methyl 3-amino-2,4,6-trimethylphenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 205517-06-2
3-amino-2,4,6-trimethylphenylacetonitrile

: 205516-96-7
methyl 3-amino-2,4,6-trimethylphenylacetate

Guidance literature:: With sulfuric acid; In methanol;

Reference yield:

: 34688-71-6
mesitylacetonitrile

: 205516-96-7
methyl 3-amino-2,4,6-trimethylphenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / 70 percent HNO₃; conc. H₂SO₄; AcOH / 1 h

2: 79 percent / aq. NH₄Cl; Zn / methanol / 4 h

3: conc. H₂SO₄ / 15 h / Heating

With sulfuric acid; nitric acid; ammonium chloride; acetic acid; zinc; In methanol; 1: Nitration / 2: Reduction / 3: methanolysis;
DOI:10.1021/jm9900063

Reference yield:

: 205517-05-1
2,4,6-trimethyl-3-nitrobenzeneacetonitrile

: 205516-96-7
methyl 3-amino-2,4,6-trimethylphenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / aq. NH₄Cl; Zn / methanol / 4 h

2: conc. H₂SO₄ / 15 h / Heating

With sulfuric acid; ammonium chloride; zinc; In methanol; 1: Reduction / 2: methanolysis;
DOI:10.1021/jm9900063