2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose

Base Information

Chemical Name:2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose
CAS No.:1385789-85-4
Molecular Formula:C₂₀H₂₃N₃O₁₂S
Molecular Weight:529.482
Hs Code.:

Synonyms:2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose

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Chemical Property of 2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose

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Technology Process of 2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose

There total 1 articles about 2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 343925-61-1
(2R,3S,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-mercaptotetrahydro-2H-pyran-3,4-diyl diacetate

: 1385789-85-4
2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2ob25429h

Reference yield: 34.0%

: 1385789-85-4
2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose

: 1228577-53-4
2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-α-D-glucopyranose

Guidance literature:: With water; In methanol; acetone; at 20 ℃; for 1h;
DOI:10.1039/c2ob25429h

Reference yield:

: 1385789-85-4
2,4-dinitrophenyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranose

: 1385789-88-7
C₁₉H₁₈N₄O₁₂S₂

Guidance literature:: Multi-step reaction with 2 steps

1: water / methanol; acetone / 1 h / 20 °C

2: MshB / dimethyl sulfoxide / 0.5 h / 30 °C / pH 7.5 / aq. buffer

With MshB; water; In methanol; dimethyl sulfoxide; acetone;
DOI:10.1039/c2ob25429h