N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide

Base Information

Chemical Name:N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide
CAS No.:171414-19-0
Molecular Formula:C₁₇H₂₀N₂O₅S
Molecular Weight:364.422
Hs Code.:

Synonyms:N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide

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Technology Process of N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide

There total 5 articles about N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 106-94-5
propyl bromide

: 171414-16-7
N-(4-methoxybenzyl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

: 171414-19-0
N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 0.5h;
DOI:10.1016/0040-4039(95)01316-A

Reference yield: 96.0%

: 1426308-72-6
N-(4-methoxybenzyl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

: 171414-19-0
N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide

Guidance literature:: With hydrogen; In methanol; at 25 ℃; for 4h; chemoselective reaction;
DOI:10.1021/ol4002448

Reference yield:

: 171414-16-7
N-(4-methoxybenzyl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

: 171414-19-0
N-(4-methoxybenzyl)-2-nitro-N-propylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide; toluene / 2 h / 20 °C / Inert atmosphere

2: hydrogen / methanol / 4 h / 25 °C

With hydrogen; potassium carbonate; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol4002448