C₃₁H₄₃N₃O₅

Base Information

Chemical Name:C₃₁H₄₃N₃O₅
CAS No.:1613626-32-6
Molecular Formula:C₃₁H₄₃N₃O₅
Molecular Weight:537.7
Hs Code.:

C<sub>31</sub>H<sub>43</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₃₁H₄₃N₃O₅

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Chemical Property of C₃₁H₄₃N₃O₅

Chemical Property:

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Technology Process of C₃₁H₄₃N₃O₅

There total 17 articles about C₃₁H₄₃N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613626-31-5
C₂₃H₃₇N₃O₃*C₂H₄O₂

: 501-53-1,94274-21-2
benzyl chloroformate

: 1613626-32-6
C₃₁H₄₃N₃O₅

Guidance literature:: With sodium carbonate; In methanol; water; at 0 - 20 ℃; for 2h;

Reference yield:

: 529-35-1
5,6,7,8-Tetrahydronaphthalen-1-ol

: 1613626-32-6
C₃₁H₄₃N₃O₅

Guidance literature:: Multi-step reaction with 17 steps

1.1: sodium hydroxide / tetrahydrofuran / 3 h / 0 - 20 °C

2.1: aluminum (III) chloride / dichloromethane / 0.17 h / 0 °C

2.2: 3 h / 0 - 20 °C

3.1: hydrogenchloride; zinc / toluene / 3 h / Reflux

4.1: pivaloyl chloride; lithium chloride; triethylamine / tetrahydrofuran / 2 h / -25 - 20 °C

5.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

5.2: -78 °C

5.3: 4 h / -78 - 27 °C

6.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1 h / 0 °C

7.1: hydrogen; palladium 10% on activated carbon / water / 16 h / 20 °C / 760.05 Torr

8.1: acetic acid; hydrogen bromide / 16 h / Reflux

9.1: acetyl chloride / 3 h / Reflux

10.1: sodium hydrogencarbonate / methanol; water / 3 h / 0 - 20 °C

11.1: pyridine / 1 h / 0 - 20 °C

12.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

13.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C

14.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 1 h / 0 °C

15.1: ammonia / methanol / 2 h / 0 - 20 °C

16.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

17.1: sodium carbonate / methanol; water / 2 h / 0 - 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; aluminum (III) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; sodium carbonate; acetic acid; triethylamine; acetyl chloride; lithium chloride; sodium hydroxide; lithium hydroxide; zinc; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 1008-19-1
5-methoxy-1,2,3,4-tetrahydro-naphthalene

: 1613626-32-6
C₃₁H₄₃N₃O₅

Guidance literature:: Multi-step reaction with 16 steps

1.1: aluminum (III) chloride / dichloromethane / 0.17 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: hydrogenchloride; zinc / toluene / 3 h / Reflux

3.1: pivaloyl chloride; lithium chloride; triethylamine / tetrahydrofuran / 2 h / -25 - 20 °C

4.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

4.2: -78 °C

4.3: 4 h / -78 - 27 °C

5.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1 h / 0 °C

6.1: hydrogen; palladium 10% on activated carbon / water / 16 h / 20 °C / 760.05 Torr

7.1: acetic acid; hydrogen bromide / 16 h / Reflux

8.1: acetyl chloride / 3 h / Reflux

9.1: sodium hydrogencarbonate / methanol; water / 3 h / 0 - 20 °C

10.1: pyridine / 1 h / 0 - 20 °C

11.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

12.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C

13.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 1 h / 0 °C

14.1: ammonia / methanol / 2 h / 0 - 20 °C

15.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

16.1: sodium carbonate / methanol; water / 2 h / 0 - 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; aluminum (III) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; sodium carbonate; acetic acid; triethylamine; acetyl chloride; lithium chloride; sodium hydroxide; lithium hydroxide; zinc; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; toluene; acetonitrile;