N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide

Base Information

Chemical Name:N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide
CAS No.:148854-65-3
Molecular Formula:C₂₀H₂₅N₅O₇S₂
Molecular Weight:511.58
Hs Code.:

N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide

Synonyms:N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide

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Chemical Property of N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide

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Technology Process of N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide

There total 1 articles about N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2651-13-0
p-acetylaminobenzenesulphonyliminodithiocarbonic acid dimethyl ester

: 25152-20-9
5'-amino-5'-deoxythymidine

: 148854-65-3
N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide

Guidance literature:: In pyridine; at 80 ℃; for 18h; Yield given;

Reference yield: 74.0%

: 52450-18-7
3'-amino-3'-deoxythymidine

: 148854-65-3
N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide

: 148854-74-4
N'-(p-acetamidophenylsulfonyl)-N-(3'-deoxythymidin-3'-yl)-N''-(5'-deoxythymidin-5'-yl)guanidine

Guidance literature:: With silver nitrate; In triethylamine; N,N-dimethyl-formamide; for 18h; Ambient temperature;

Reference yield:

: 148854-65-3
N-(4-{[1-{[(2R,3S,5R)-3-Hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-amino}-1-methylsulfanyl-meth-(Z)-ylidene]-sulfamoyl}-phenyl)-acetamide

: C₅₀H₅₄N₈O₁₃S

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / AgNO₃ / dimethylformamide; triethylamine / 18 h / Ambient temperature

2: 95 percent / pyridine / 18 h / Ambient temperature

With pyridine; silver nitrate; In triethylamine; N,N-dimethyl-formamide;