methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

Base Information

Chemical Name:methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate
CAS No.:1642568-76-0
Molecular Formula:C₂₂H₂₂N₂O₄
Molecular Weight:378.428
Hs Code.:

Synonyms:methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

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Chemical Property of methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

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Technology Process of methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

There total 4 articles about methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1631-25-0
N-cyclohexylmaleimide

: 121911-01-1
methyl-(1,2,3,4-tetrahydroisochinolin-2-yl)-acetate

: 1642568-76-0
methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

Guidance literature:: With alizarin red S; eosin Y disodium salt; In acetone; at 28 ℃; for 20h; Irradiation;
DOI:10.1016/j.tet.2021.132166

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 1642568-76-0
methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 1 h / 0 - 5 °C

2: acetic anhydride; sodium acetate / 2 h / 70 °C

3: cadmium sulphide / neat (no solvent) / 24 h / 20 °C / Irradiation; Green chemistry

With cadmium sulphide; sodium acetate; acetic anhydride; In dichloromethane;
DOI:10.1039/c8gc03297a

Reference yield:

: 24564-83-8
C₁₀H₁₅NO₃

: 1642568-76-0
methyl 10-cyclohexyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride; sodium acetate / 2 h / 70 °C

2: cadmium sulphide / neat (no solvent) / 24 h / 20 °C / Irradiation; Green chemistry

With cadmium sulphide; sodium acetate; acetic anhydride; In neat (no solvent);
DOI:10.1039/c8gc03297a